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IL-1, interleukin-1

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Peptides were loaded with 0.1% TFA in water at 2.5 l/minute for 10 minutes onto a trapping column (3 cm 150 m, Bischoff ProntoSIL C18-AQ, 3 m, 200 resin) and then separated on a New Objective PicoChip analytical column (10 cm 75 m, ProntoSIL C18-AQ, 3 m, 200 resin)

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A futility analysis showed that the enzalutamide control arm performed better than historical controls, and similar to the masofaniten-enzalutamide combination, and thus was unlikely to achieve the trials primary endpoint